Reactivity of hydrazinium hydrazinecarboxylatesynthesis of 4-amino-3, 5-dimethyl-l, 2, 4-triazole

J J VITTAL, V B ANGADI, K C PATIL

Abstract


The reaction between hydrazinum hydrazinccarboxylate, N2H5+ and accetonitrile at ambient conditions produces a white solid computnd which was found to be 4-amino-3, 5-dimethyl-1 2, 4-triazole by chemical analysis, IR (1H and 1 3C) NMR spectra and mass spectral fragmentation pattern. A probable mechanism for the formation of triazole is proposed. The preparative method is standardized.


Keywords


Hydrazinium hydrazinecarboxylate; and 4-amino-3; 5-dimethyi-1,2,4-triazole.

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